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I put my wetsuit in first so that it had the most contact with the water. Make sure you press all the velcro parts together with their counterparts or else the tabs will chew up your bathing suit and other neoprene stuff if it comes into contact with it.
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Next everything else that I wear for skiing went in: my bathing suits, board shorts, gloves, glove liners, lifejacket, and heat shirt.
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Everything tries to float, so you have to squash it down to get water on it. I left it in for a couple of hours, but every once in a while, I swished it around more so that the floating parts would make better contact. I rearranged once and flipped my wetsuit and life jacket over so that a different side was facing up. When you’re done, rinse it thoroughly. I did this by letting out the water with my stuff still in the tub, then filling it up with clear water and swishing it around. I left it for another 30 minutes, then did the same thing twice more–3 tubs of clean water in all. You can tell when the water is good because it doesn’t feel slippery to the touch (one of the effects of baking soda in water). Then I hung it all up to dry. Worked like a charm; no smell at all! It’s ready to store away until next season.